µ-XRF Analysis of Trace Elements in Lapis Lazuli-Forming Minerals for a Provenance Study

Microscopy and Microanalysis : the Official Journal of Microscopy Society of America, Microbeam Analysis Society, Microscopical Society of Canada
Debora AngeliciGloria Vaggelli

Abstract

This paper presents new developments on the provenance study of lapis lazuli started by our group in 2008: during the years a multi-technique approach has been exploited to obtain minero-petrographic characterization and creation of a database considering only rock samples of known provenance. Since the final aim of the study is to develop a method to analyze archeological findings and artworks made with lapis lazuli in a completely non-invasive way, ion beam analysis techniques were employed to trace the provenance of the raw material used for the production of artifacts. Continuing this goal and focusing the analysis on determination of more significant minero-chemical markers for the provenance study of trace elements in different minerals, the method was extended with the use of micro X-ray fluorescence (µ-XRF), to test the potential of the technique for this application. The analyzes were focused on diopside and pyrite in lapis lazuli samples of known provenance (Afghanistan, Tajikistan, and Siberia). In addition, µ-XRF data were compared with micro proton-induced X-ray emission (µ-PIXE) results to verify the agreement between the two databases and to compare the analytical performance of both techniques for this application.

References

Aug 26, 2009·Analytical and Bioanalytical Chemistry·Alessandro Lo GiudiceElisa Conz
Oct 13, 2009·Analytical and Bioanalytical Chemistry·D SokarasV Kantarelou
May 28, 2011·Microscopy and Microanalysis : the Official Journal of Microscopy Society of America, Microbeam Analysis Society, Microscopical Society of Canada·Silvia Calusi
May 31, 2012·Analytical and Bioanalytical Chemistry·Alessandro Lo GiudiceGiovanni Pratesi

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Citations

May 11, 2016·Microscopy and Microanalysis : the Official Journal of Microscopy Society of America, Microbeam Analysis Society, Microscopical Society of Canada·Luigi GerminarioClaudio Mazzoli

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