3D Nanoarchitecture of Polyaniline-MoS2 Hybrid Material for Hg(II) Adsorption Properties

Polymers
Hilal AhmadAli Alsalme

Abstract

We report the facile hydrothermal synthesis of polyaniline (PANI)-modified molybdenum disulfide (MoS2) nanosheets to fabricate a novel organic-inorganic hybrid material. The prepared 3D nanomaterial was characterized by field emission scanning electron microscopy, high-resolution transmission electron microscopy, energy-dispersive X-ray spectroscopy and X-ray diffraction studies. The results indicate the successful synthesis of PANI-MoS2 hybrid material. The PANI-MoS2 was used to study the extraction and preconcentration of trace mercury ions. The experimental conditions were optimized systematically, and the data shows a good Hg(II) adsorption capacity of 240.0 mg g-1 of material. The adsorption of Hg(II) on PANI-MoS2 hybrid material may be attributed to the selective complexation between the-S ion of PANI-MoS2 with Hg(II). The proposed method shows a high preconcentration limit of 0.31 µg L-1 with a preconcentration factor of 640. The lowest trace Hg(II) concentration, which was quantitatively analyzed by the proposed method, was 0.03 µg L-1. The standard reference material was analyzed to determine the concentration of Hg(II) to validate the proposed methodology. Good agreement between the certified and observed values indic...Continue Reading

References

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Citations

Aug 11, 2021·Polymers·Jesús-María García-Martínez, Emilia P Collar

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Methods Mentioned

BETA
X-ray
2 hybrid
2
transmission electron microscopy
infrared spectroscopy

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