A high-throughput method for determining chloramphenicol residues in poultry, egg, shrimp, fish, swine and bovine using LC-ESI-MS/MS

Journal of Separation Science
Silvia Regina Rocha SiqueiraFelix Guillermo Reyes Reyes

Abstract

A LC-ESI-MS/MS method for determining chloramphenicol residues in fish, shrimp, poultry, eggs, bovine and swine was developed and validated. The samples were extracted with a phosphate extraction solution followed by liquid-liquid extraction with ethyl acetate. The LC was performed on a C18 column at room temperature. For all the matrices, the analytical curves showed r values and recoveries higher than 0.99 and 50%, respectively. The accuracy values lay between 85 and 120% and the precision was lower than 20%. The LOQ was 0.1 ng/g. The method was employed to analyze samples collected in Brazil.

References

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Mar 5, 2004·Journal of Agricultural and Food Chemistry·Evangelos GikasAnthony Tsarbopoulos
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Citations

Oct 20, 2011·Food Additives & Contaminants. Part A, Chemistry, Analysis, Control, Exposure & Risk Assessment·Hong XuLishuang Liu
Jul 21, 2011·Luminescence : the Journal of Biological and Chemical Luminescence·Xiao Feng YangHong Qun Luo
Sep 11, 2014·Food Additives & Contaminants. Part A, Chemistry, Analysis, Control, Exposure & Risk Assessment·Felix E MbodiJ Kabir
Nov 14, 2016·Talanta·Letícia R GuidiMaria Beatriz A Gloria
Sep 19, 2017·Journal of Environmental Science and Health. Part. B, Pesticides, Food Contaminants, and Agricultural Wastes·Muhammad I ChughtaiTerence Fodey
Aug 12, 2009·Analytical and Bioanalytical Chemistry·Yu-Chang TyanJentaie Shiea
Nov 22, 2013·Journal of Mass Spectrometry : JMS·Élida AlechagaM Teresa Galceran
Dec 1, 2020·Japanese Journal of Infectious Diseases·Paweena KongsananChanwit Tribuddharat

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