Adsorption of lead ions from wastewater using nano silica spheres synthesized on calcium carbonate templates

Heliyon
Milton ManyangadzeTirivaviri A Mamvura

Abstract

Lead is a heavy metal that is bio accumulative and non-biodegradable that poses a threat to our health when it exists in excess in our bloodstream. It has found its way into wastewater from mostly chemical industrial processes. In this article, we investigated the adsorption and hence removal of lead (II) ions from wastewater in order to purify it for re-use in industrial processes or for plant and animal use. We synthesized nano silica hollow spheres (NSHS) and used them as adsorbents to remove lead ions from wastewater. When we characterized the NSHS using X-Ray diffraction, the amorphous nature of silica was evident with average crystal size of 39.5 nm. Scanning electron microscopy was used to determine the morphology of the adsorbent and the particles were found to be spherical in shape within a size range of 100-200 nm. Thermogravimetric analysis was used to determine the mass loss of NSHS which was ~2% at 800 °C. Our experimental results from adsorption studies showed that there was a linear relationship between temperature (27-60 °C) and adsorption efficiency and an inverse relationship between initial metal concentration (50-300 mg/L) and adsorption efficiency. At a maximum temperature of 60 °C and maximum initial metal...Continue Reading

References

Jul 26, 2011·Journal of Hazardous Materials·Sarika SinghD Bahadur
Nov 23, 2019·Journal of Hazardous Materials·Tina KeglIrena Ban
Jan 27, 2020·Environmental Monitoring and Assessment·Uriel Fernando Carreño SayagoAlexander Garcia Mariaca

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Methods Mentioned

BETA
X-Ray
Scanning Electron Microscopy
gel by filtration
Atomic Absorption Spectroscopy

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