PMID: 11312819Apr 21, 2001Paper

Analysis of limonoid glucosides from citrus by electrospray ionization liquid chromatography-mass spectrometry

Journal of Agricultural and Food Chemistry
Thomas K SchochShin Hasegawa

Abstract

An electrospray ionization liquid chromatography-mass spectrometry (ESI-LC-MS) method for the detection and quantitation of limonoid glucosides has been developed. Negative ions [M - H(+)](-) characteristic of six limonoid glucosides can be detected and quantified from selected ion monitoring chromatograms using carminic acid as an internal standard. The described method has been applied to the analysis of limonoid glucoside content in various liquid and solid Citrus spp. samples as well as complex mixtures of partially purified limonoid glucosides. Rapid and sensitive qualitative screening of samples for limonoid glucosides can also be accomplished with slight modifications of the method.

Citations

Nov 16, 2001·Phytochemical Analysis : PCA
Jun 18, 2011·Journal of the Science of Food and Agriculture·Andrew P BreksaMichelle Lee Yuen
Dec 18, 2001·Journal of Mass Spectrometry : JMS
Nov 11, 2003·Rapid Communications in Mass Spectrometry : RCM·Qingguo TianBhimanagouda S Patil
Dec 21, 2010·Journal of Separation Science·Guddadarangavvanahally K JayaprakashaBhimanagouda S Patil
Jun 5, 2007·Journal of Agricultural and Food Chemistry·Andrew P Breksa, Phil Ibarra
Dec 18, 2001·Journal of Agricultural and Food Chemistry·R J Braddock, C R Bryan
Jan 9, 2004·Analytical Chemistry·Qingguo Tian, Steven J Schwartz
Sep 26, 2007·Journal of Agricultural and Food Chemistry·Gary D Manners
May 25, 2006·Journal of Agricultural and Food Chemistry·Andrew P Breksa, Gary D Manners

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