Assessment of the Suitability of the One-Step Hydrothermal Method for Preparation of Non-Covalently/Covalently-Bonded TiO₂/Graphene-Based Hybrids

Nanomaterials
Ewelina Kusiak-NejmanAntoni W Morawski

Abstract

A hybrid nanocomposites containing nanocrystalline TiO₂ and graphene-related materials (graphene oxide or reduced graphene oxide) were successfully prepared by mechanical mixing and the hydrothermal method in the high-pressure atmosphere. The presented X-ray photoelectron spectroscopy (XPS) study and quantitative elemental analysis confirm similar content of carbon in graphene oxide GO (52 wt% and 46 wt%, respectively) and reduced graphene oxide rGO (92 wt% and 98 wt%, respectively). No chemical interactions between TiO₂ and GO/rGO was found. TiO₂ nanoparticles were loaded on GO or rGO flakes. However, Fourier transform infrared-diffuse reflection spectroscopy (FTIR/DRS) allowed finding peaks characteristic of GO and rGO. XPS study shows that since the concentration of TiO₂ in the samples was no less than 95 wt%, it was assumed that the interactions between TiO₂ and graphene should not influence the lower layers of titanium atoms in the TiO₂ and they occurred as Ti4+ ions. Hydrothermal treatment at 200 °C did not cause the reduction of GO to rGO in TiO₂-GO nanocomposites. In general, the one-step hydrothermal method must be considered to be inefficient for preparation of chemically-bonded composites synthesized from commerciall...Continue Reading

References

Jan 1, 2010·ACS Nano·Hao ZhangJinghong Li
Jul 4, 2012·Nanoscale Research Letters·Yao YaoXiaoyu Li
May 21, 2013·International Journal of Nanomedicine·Sangiliyandi GurunathanJin-Hoi Kim
Jan 24, 2014·Nature Chemistry·Priyank V KumarJeffrey C Grossman
May 16, 2015·Scientific Reports·Sina AbdolhosseinzadehHyoung Seop Kim

❮ Previous
Next ❯

Methods Mentioned

BETA
X-ray
scanning
thermal treatment
thermal reduction

Software Mentioned

POLICE

Related Concepts

Trending Feeds

COVID-19

Coronaviruses encompass a large family of viruses that cause the common cold as well as more serious diseases, such as the ongoing outbreak of coronavirus disease 2019 (COVID-19; formally known as 2019-nCoV). Coronaviruses can spread from animals to humans; symptoms include fever, cough, shortness of breath, and breathing difficulties; in more severe cases, infection can lead to death. This feed covers recent research on COVID-19.

Blastomycosis

Blastomycosis fungal infections spread through inhaling Blastomyces dermatitidis spores. Discover the latest research on blastomycosis fungal infections here.

Nuclear Pore Complex in ALS/FTD

Alterations in nucleocytoplasmic transport, controlled by the nuclear pore complex, may be involved in the pathomechanism underlying multiple neurodegenerative diseases including Amyotrophic Lateral Sclerosis and Frontotemporal Dementia. Here is the latest research on the nuclear pore complex in ALS and FTD.

Applications of Molecular Barcoding

The concept of molecular barcoding is that each original DNA or RNA molecule is attached to a unique sequence barcode. Sequence reads having different barcodes represent different original molecules, while sequence reads having the same barcode are results of PCR duplication from one original molecule. Discover the latest research on molecular barcoding here.

Chronic Fatigue Syndrome

Chronic fatigue syndrome is a disease characterized by unexplained disabling fatigue; the pathology of which is incompletely understood. Discover the latest research on chronic fatigue syndrome here.

Evolution of Pluripotency

Pluripotency refers to the ability of a cell to develop into three primary germ cell layers of the embryo. This feed focuses on the mechanisms that underlie the evolution of pluripotency. Here is the latest research.

Position Effect Variegation

Position Effect Variagation occurs when a gene is inactivated due to its positioning near heterochromatic regions within a chromosome. Discover the latest research on Position Effect Variagation here.

STING Receptor Agonists

Stimulator of IFN genes (STING) are a group of transmembrane proteins that are involved in the induction of type I interferon that is important in the innate immune response. The stimulation of STING has been an active area of research in the treatment of cancer and infectious diseases. Here is the latest research on STING receptor agonists.

Microbicide

Microbicides are products that can be applied to vaginal or rectal mucosal surfaces with the goal of preventing, or at least significantly reducing, the transmission of sexually transmitted infections. Here is the latest research on microbicides.

© 2022 Meta ULC. All rights reserved