Basic Insights into Tunable Graphene Hydrogenation

Journal of the American Chemical Society
Ricarda A SchäferAndreas Hirsch

Abstract

The hydrogenation and deuteration of graphite with potassium intercalation compounds as starting materials were investigated in depth. Characterization of the reaction products (hydrogenated and deuterated graphene) was carried out by thermogravimetric analysis coupled with mass spectrometry (TG-MS) and statistical Raman spectroscopy (SRS) and microscopy (SRM). The results reveal that the choice of the hydrogen/deuterium source, the nature of the graphite (used as starting material), the potassium concentration in the intercalation compound, and the choice of the solvent have a great impact on the reaction outcome. Furthermore, it was possible to prove that both mono- and few-layer hydrogenated/deuterated graphene can be produced.

References

Mar 1, 2003·Science·Lisa M ViculisRichard B Kaner
Mar 25, 2011·Nature Chemistry·Jan M EnglertAndreas Hirsch
Oct 18, 2012·Journal of the American Chemical Society·Zhiqiang YangW E Billups
Nov 28, 2012·Angewandte Chemie·Ricarda A SchäferAndreas Hirsch
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Citations

Mar 23, 2017·Journal of the American Chemical Society·Gonzalo AbellánAndreas Hirsch
May 10, 2017·Accounts of Chemical Research·Elena VishnyakovaW Edward Billups
Jan 14, 2017·Chemical Communications : Chem Comm·Chengmin JiangAngel A Martí
Feb 22, 2017·Nanoscale·Stephen A HodgeMilo S P Shaffer
Jul 14, 2017·Chemical Society Reviews·Giovanni BottariTomás Torres
Oct 27, 2017·Chemistry : a European Journal·Jiri SturalaZdeněk Sofer
May 10, 2017·Nature Communications·Philipp VeceraAndreas Hirsch
Mar 7, 2020·Chemistry : a European Journal·Heather AuMilo S P Shaffer
Aug 19, 2020·Angewandte Chemie·Konstantin Felix EdelthalhammerAndreas Hirsch
Aug 2, 2017·Journal of the American Chemical Society·Daniela DaslerAndreas Hirsch
Jun 12, 2019·Accounts of Chemical Research·Tao WeiHirsch Andreas

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