Characterization, molecular modeling and antimicrobial activity of metal complexes of tridentate Schiff base derived from 5-acetyl-4-hydroxy-2H-1,3-thiazine-2,6(3H)-dione and 2-aminophenol

Spectrochimica Acta. Part A, Molecular and Biomolecular Spectroscopy
Omima M I Adly

Abstract

Metal complexes of Ni(II), Co(II), Cd(II), VO(IV) and UO(2)(VI) as well as several Cu(II) salts, including Cl(-),NO(3)(-),AcO(-),ClO(4)(-) and SO(4)(-2) with a tridentate O(2)N donor Schiff base ligand (H(2)L), synthesized by condensation of 5-acetyl-4-hydroxy-2H-1,3-thiazine-2,6(3H)-dione with 2-aminophenol, were prepared and characterized on the basis of elemental analyses, spectral, magnetic, molar conductance and thermal gravimetric analysis. Square planar, tetrahedral and octahedral geometries have been assigned to the prepared complexes. Molecular parameters of the ligand and its metal complexes have been calculated and correlated with the experimental data, and the changes of bond lengths are linearly correlated with IR data. The antimicrobial activities of the synthesized compounds were tested in vitro against the sensitive organisms Staphylococcus aureus as Gram positive bacteria, Proteus vulgaris as Gram negative bacteria and Candida albicans as fungus strain, and the results are discussed.

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Citations

Jan 16, 2015·Spectrochimica Acta. Part A, Molecular and Biomolecular Spectroscopy·A TahaMagdy Shebl
Aug 19, 2016·Molecules : a Journal of Synthetic Chemistry and Natural Product Chemistry·Syed Lal Badshah, Abdul Naeem
Aug 24, 2021·Acta Crystallographica. Section E, Crystallographic Communications·R SribalaR V Krishnakumar

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