Chitosan Modified Cationic Polyacrylamide Initiated by UV-H2 O2 for Sludge Flocculation and New Insight on the Floc Characteristics Study

Polymers
Jie ChenBingzhi Liu

Abstract

In the present study, a novel graft modified flocculant CTS-g-PAMD was synthesized and applied to conduct sludge conditioning and dewatering. CTS-g-PAMD was copolymerized with AM, DMC and chitosan (CTS) under UV-H2O2 initiation. In addition, the effects of single factor experiments on the molecular weight (MW) CTS grafting efficiency (GE) of CTS-g-PAMD were determined and the optimal copolymerization conditions were achieved. The GE of CTS-g-PAMD reached 91.1% and the MW was 4.82 × 106 Da. As revealed from the characterized results of Fourier-transform infrared spectra (FT-IR), 1H/ NMR, X-ray diffraction (XRD), scanning electron microscopic (SEM) and X-ray photoelectron spectroscopy (XPS), the successful synthesis of CTS-g-PAMD was confirmed, which is considered to be conducive to explaining sludge dewatering performance. Under the optimal conditions (pH = 7.0, flocculant dosage = 35 mg/L), the best flocculating performance (FCMC: 73.7%; SRF: 4.7 × 1012 m·kg-1, turbidity: 9.4 NTU) and large and dense sludge flocs (floc size d50 = 379.142 µm, floc fractal dimension Df = 1.58) were formed. The DMC and CTS chain segments exhibiting cationic properties significantly improved the positive charge density and enhanced the electrical p...Continue Reading

References

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Oct 13, 2010·Langmuir : the ACS Journal of Surfaces and Colloids·Ming FangGuohua Chen
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Methods Mentioned

BETA
X-ray

Software Mentioned

Pro Plus
Image
PAMD

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