Comparison of micro-scale simultaneous distillation-extraction and stir bar sorptive extraction for the determination of volatile organic constituents of grape juice

Journal of Chromatography. a
Darren J Caven-Quantrill, Alan J Buglass

Abstract

Traditional micro-scale simultaneous distillation-extraction (SDE) and stir bar sorptive extraction (SBSE) were compared for their effectiveness in the extraction of volatile organic compounds in a synthetic grape juice and a real grape juice (Huxelrebe, a variety of half Muscat ancestry) from an English vineyard. The novel immersion-mode SBSE method, using stir bars with PDMS sorbent, was optimised using the synthetic grape juice. Although mean percent relative recoveries and reproducibilities (%CV) of the SBSE method were inferior to SDE (28.4 and 8.5%, respectively, against 86.9 and 6.3%), the former method proved to be significantly more sensitive: 126 aroma compounds in Huxelrebe grape juice were identified using SBSE, against 98 using SDE. This allowed the identification of a number of volatile components that have not been reported previously in the juice or wine from the grapes of Muscat varieties.

References

Feb 13, 2003·Journal of Chromatography. a·Jan C R DemyttenaereNorbert De Kimpe
Feb 7, 2004·Journal of Chromatography. a·Juan DíezCarmelo G Barroso

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Citations

Aug 27, 2011·Journal of Agricultural and Food Chemistry·Mark A SeftonDennis K Taylor
Apr 14, 2015·Free Radical Research·H StutzP M Eckl
Jul 14, 2012·Analytica Chimica Acta·Henryk H JeleńMariusz Dziadas
Feb 23, 2007·Journal of Chromatography. a·Kathy RidgwayRoger M Smith
Jan 24, 2007·Journal of Chromatography. a·Frank David, Pat Sandra
Jan 31, 2012·Analytica Chimica Acta·Anna BanelBogdan Zygmunt
Jan 31, 2012·Talanta·M Rosario SalinasTeresa Garde-Cerdán
Jul 7, 2009·Talanta·E Sánchez-PalomoM S Pérez-Coello
Jul 28, 2016·Journal of Separation Science·Carla HerreraEnrique Durán-Guerrero
Aug 22, 2012·Journal of Chromatographic Science·Huayuan LuoJunsong Zhang
Dec 21, 2018·Chemistry Central Journal·Kevin McAdamBrad Rodu
Oct 12, 2007·Journal of Agricultural and Food Chemistry·Berhane T WeldegergisAndrew M Crouch
Nov 26, 2020·Food Research International·Sandra Marín-San RománTeresa Garde-Cerdán

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