Determination of acrylamide in foods by pressurized fluid extraction and liquid chromatography-tandem mass spectrometry used for a survey of Spanish cereal-based foods

Food Additives and Contaminants
Vicent YusàAgustín Pastor

Abstract

An automated and rapid method for the determination of acrylamide in different food products is presented. The method involves pressurized fluid extraction (PFE) of foods with acetonitrile and precipitation with Carrez reagents. The final extract is analysed by liquid chromatography coupled to electrospray ionization tandem mass spectrometry (ESI-MS-MS). The main parameters affecting the performance of ESI-MS-MS and PFE were optimized using a design of experiments approach. The limit of quantification of the method was 5 microg kg(-1), and recoveries from incurred samples ranged between 93 and 101%. The accuracy was evaluated using the reference test materials FAPAS T3002, T3005 and T3011. Using the optimized method, 62 food samples of potato chips, snacks, biscuits, breakfast cereals and crisp bread sampled from Valencia, Spain, supermarkets were surveyed for acrylamide levels. The levels were similar to those reported in the European Union and USA.

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Citations

Aug 4, 2007·Analytical and Bioanalytical Chemistry·Thomas WenzlVural Gökmen
Jul 21, 2011·Analytical and Bioanalytical Chemistry·Rudolf KrskaDon Forsyth
Dec 29, 2013·Journal of Agricultural and Food Chemistry·Antonio Dario TroiseVincenzo Fogliano
Nov 23, 2006·Food Additives and Contaminants·C SoaresJ Fernandes
Apr 25, 2007·Food Additives and Contaminants·Jose A Rufian-HenaresFrancisco J Morales
Dec 17, 2014·Food Additives & Contaminants. Part B, Surveillance·Deborah PacettiPaolo Lucci
Nov 14, 2014·Critical Reviews in Analytical Chemistry·Abdalla A ElbashirHassan Y Aboul-Enein
Dec 19, 2013·Critical Reviews in Food Science and Nutrition·Ioannis S Arvanitoyannis, Niki Dionisopoulou
Jul 26, 2006·Molecular Nutrition & Food Research·José A Rufián-HenaresFrancisco J Morales
Dec 1, 2006·Journal of Mass Spectrometry : JMS
Feb 19, 2019·Food Additives & Contaminants. Part B, Surveillance·Yen Dao HaiGiang Truong Le
Oct 21, 2017·Food Additives & Contaminants. Part A, Chemistry, Analysis, Control, Exposure & Risk Assessment·Nail AltunayRamazan Gürkan
Sep 29, 2018·Food Science and Biotechnology·Mohammad Rizwan KhanSulaiman Mohammed Alfadul
Feb 7, 2021·Environmental Science and Pollution Research International·Neda Mollakhalili-MeybodiMasoumeh Arab
Mar 10, 2016·Journal of the American Society for Mass Spectrometry·Elizabeth S HechtDavid C Muddiman

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Methods Mentioned

BETA
chips

Software Mentioned

MINITAB

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