Double-resonance magic angle coil spinning

Journal of Magnetic Resonance
Munehiro Inukai, Kazuyuki Takeda

Abstract

We present an extension of magic angle coil spinning (MACS) solid-state NMR spectroscopy to double-resonance experiments, enabling implementation of powerful double-resonance solid-state NMR methodologies including cross polarization, proton decoupling, and two-dimensional correlation spectroscopy etc., while still enjoying the merits that are intrinsic to MACS, such as high concentration sensitivity, eliminated magnetic susceptibility-induced field distortion, and an easy-to-use approach with the conventional and widespread hardware.

Citations

Aug 23, 2012·Environmental Science & Technology·Andre J SimpsonRonald Soong
Jul 8, 2015·Journal of Magnetic Resonance·Kazuyuki TakedaK Takegoshi
Aug 22, 2016·Journal of Magnetic Resonance·J A Lehmann-HornD Sakellariou
Dec 25, 2010·Chemical Communications : Chem Comm·Pedro M AguiarDimitris Sakellariou

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