Effect of an experimental zirconia-silica coating technique on micro tensile bond strength of zirconia in different priming conditions

Dental Materials : Official Publication of the Academy of Dental Materials
Chenfeng ChenAlbert J Feilzer

Abstract

This study aimed to evaluate the adhesive properties of a MDP-containing resin cement to a colored zirconia ceramic, using an experimental zirconia-silica coating technique with different priming conditions. 18 zirconia ceramic discs (Cercon base colored) were divided into two groups: the control group and the experimental zirconia-silica coating group. Specimens in each group were further divided into 3 subgroups (n = 3) according to the priming conditions: no primer, a MDP-containing primer (ED Primer II) or a silane coupling primer (RelyX™ Ceramic Primer). Then resin-composite discs (Filtek™ Z250) were bonded to the treated surface using a MDP-containing resin cement (Panavia F 2.0). The bi-layered specimens were cut into microbars and 20 microbars were randomly selected from each specimen, half of which were stored in 37°C water bath for 24h, and the other half were stored for 30 days. After water storage, the samples were exposed to a micro tensile bond strength test (MTBS). The results were analyzed by ANOVA, while the fracture surfaces were examined by SEM. After 24h water storage, zirconia-silica coating followed by silanization showed a significantly (P<0.001) higher MTBS value 45.0 (10.9)MPa. Water storage affected (P...Continue Reading

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