Fabric phase sorptive extraction followed by UHPLC-MS/MS for the analysis of benzotriazole UV stabilizers in sewage samples

Analytical and Bioanalytical Chemistry
Sarah Montesdeoca-EspondaJosé Juan Santana-Rodríguez

Abstract

A fast and sensitive sample preparation strategy using fabric phase sorptive extraction followed by ultra-high-performance liquid chromatography and tandem mass spectrometry detection has been developed to analyse benzotriazole UV stabilizer compounds in aqueous samples. Benzotriazole UV stabilizer compounds are a group of compounds added to sunscreens and other personal care products which may present detrimental effects to aquatic ecosystems. Fabric phase sorptive extraction is a novel solvent minimized sample preparation approach that integrates the advantages of sol-gel derived hybrid inorganic-organic nanocomposite sorbents and the flexible, permeable and hydrophobic surface chemistry of polyester fabric. It is a highly sensitive, fast, efficient and inexpensive device that can be reused and does not suffer from coating damage, unlike SPME fibres or stir bars. In this paper, we optimized the extraction of seven benzotriazole UV filters evaluating the majority of the parameters involved in the extraction process, such as sorbent chemistry selection, extraction time, back-extraction solvent, back-extraction time and the impact of ionic strength. Under the optimized conditions, fabric phase sorptive extraction allows enrichme...Continue Reading

References

Mar 19, 2005·Environmental Science & Technology·Marianne E BalmerThomas Poiger
May 19, 2006·Journal of Colloid and Interface Science·A Venkateswara RaoG M Pajonk
Feb 12, 2009·Analytical and Bioanalytical Chemistry·Sarah Montesdeoca EspondaJosé Juan Santana Rodríguez
Apr 7, 2011·The Journal of Toxicological Sciences·Joon-Woo KimShinsuke Tanabe
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Mar 5, 2013·Analytica Chimica Acta·Habib BagheriMehrnoush Naderi

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Citations

Oct 2, 2020·Food Additives & Contaminants. Part A, Chemistry, Analysis, Control, Exposure & Risk Assessment·Babra MoyoNikita T Tavengwa
Mar 16, 2019·Molecules : a Journal of Synthetic Chemistry and Natural Product Chemistry·Ramandeep KaurVictoria F Samanidou
Jun 6, 2020·Molecules : a Journal of Synthetic Chemistry and Natural Product Chemistry·José GrauAlberto Chisvert
Dec 8, 2020·The Science of the Total Environment·Sarah Montesdeoca-EspondaJosé Juan Santana-Rodríguez
Feb 11, 2021·Molecules : a Journal of Synthetic Chemistry and Natural Product Chemistry·Abuzar Kabir, Victoria Samanidou
May 16, 2019·Journal of Proteome Research·Alexandra TarabolettiFrederic Zenhausern

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