Facile synthesis of the tridecameric Al13 nanocluster Al13(mu3-OH)6(mu2-OH)18(H2O)24(NO3)15

Inorganic Chemistry
Jason T GatlinDarren W Johnson

Abstract

Treatment of aluminum nitrate with an organic nitroso-containing compound yields the "flat", tridecameric nanocluster Al 13(mu 3-OH) 6(mu 2-OH) 18(H 2O) 24(NO 3) 15 ( Al 13 ) in good yield on a preparative scale under ambient conditions. Synthetic procedures yielding two different single-crystal forms of the Al 13 cation with two varying counterion compositions are described.

References

Feb 12, 2000·Angewandte Chemie·L AlloucheF Taulelle
Mar 10, 2005·Journal of the American Chemical Society·Elisabeth RatherDarren W Johnson
Jul 7, 2005·Inorganic Chemistry·William H CaseyBrian L Phillips
Jan 13, 2006·Chemical Reviews·William H Casey

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Citations

Sep 10, 2011·Inorganic Chemistry·Zhong SunShuangyan Du
Dec 4, 2012·International Journal of Molecular Sciences·Xianlong WangHui Zhao
Oct 30, 2013·Proceedings of the National Academy of Sciences of the United States of America·Wei WangDouglas A Keszler
Jan 15, 2015·Inorganic Chemistry·Daniel K UnruhTori Z Forbes
Nov 1, 2008·Angewandte Chemie·Zachary L MensingerDarren W Johnson
Jul 2, 2015·Angewandte Chemie·Dana ReusserAlexandra Navrotsky
Sep 29, 2011·Chemical Society Reviews·Zachary L MensingerDarren W Johnson
Nov 15, 2011·Dalton Transactions : an International Journal of Inorganic Chemistry·Xiaoyan JinShuping Bi
Jul 5, 2013·Dalton Transactions : an International Journal of Inorganic Chemistry·Zhong SunLi Wang
Sep 28, 2018·ACS Applied Materials & Interfaces·Cory K PerkinsDouglas A Keszler
Oct 20, 2017·Inorganic Chemistry·Joseph W BennettSara E Mason

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