Fast acquisition of multidimensional NMR spectra of solids and mesophases using alternative sampling methods

Magnetic Resonance in Chemistry : MRC
Philippe LesotOlivier Lafon

Abstract

Unique information about the atom-level structure and dynamics of solids and mesophases can be obtained by the use of multidimensional nuclear magnetic resonance (NMR) experiments. Nevertheless, the acquisition of these experiments often requires long acquisition times. We review here alternative sampling methods, which have been proposed to circumvent this issue in the case of solids and mesophases. Compared to the spectra of solutions, those of solids and mesophases present some specificities because they usually display lower signal-to-noise ratios, non-Lorentzian line shapes, lower spectral resolutions and wider spectral widths. We highlight herein the advantages and limitations of these alternative sampling methods. A first route to accelerate the acquisition time of multidimensional NMR spectra consists in the use of sparse sampling schemes, such as truncated, radial or random sampling ones. These sparsely sampled datasets are generally processed by reconstruction methods differing from the Discrete Fourier Transform (DFT). A host of non-DFT methods have been applied for solids and mesophases, including the G-matrix Fourier transform, the linear least-square procedures, the covariance transform, the maximum entropy and th...Continue Reading

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Citations

Jun 18, 2016·Carbohydrate Polymers·Flávio Vinicius Crizóstomo Kock, Luiz Alberto Colnago
Jul 8, 2020·Chemphyschem : a European Journal of Chemical Physics and Physical Chemistry·Boris GouilleuxPhilippe Lesot
Feb 27, 2021·Progress in Nuclear Magnetic Resonance Spectroscopy·David A Snyder
Jun 13, 2019·Solid State Nuclear Magnetic Resonance·Andrew G M RankinOlivier Lafon
Mar 5, 2020·Progress in Nuclear Magnetic Resonance Spectroscopy·Philippe LesotOlivier Lafon

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