Fingerprint analysis of Resina Draconis by ultra-performance liquid chromatography

Chemistry Central Journal
Yudi XueTao Yi

Abstract

Resina Draconis, a bright red resin derived from Dracaena cochinchinensis, is a traditional medicine used in China. To improve its quality control approach, an ultra-performance liquid chromatography (UPLC) fingerprint method was developed for rapidly evaluating the quality of Resina Draconis. The precision, repeatability and stability of the proposed UPLC method were validated in the study. Twelve batches of Resina Draconis samples from various sources were analyzed by the present UPLC method. Common peaks in the chromatograms were adopted to calculate their relative retention time and relative peak area. The chromatographic data were processed by Similarity Evaluation System for Chromatographic Fingerprint of Traditional Chinese Medicine software (Version 2004 A) for similarity analysis. The present UPLC method demonstrated a satisfactory precision, repeatability and stability. The analysis time of the present UPLC method was shortened to 30 min, compared with that of the conventional HPLC method was 50 min. The similarities of the 12 Resina Draconis samples were 0.976, 0.993, 0.955, 0.789, 0.989, 0.995, 0.794, 0.994, 0.847, 0.987, 0.997, 0.986, respectively, which indicated that the samples were certainly regionally differen...Continue Reading

References

Mar 26, 2011·Analytica Chimica Acta·Christophe TistaertYvan Vander Heyden
Jun 23, 2011·Frontiers of Medicine·Huimin GaoZhongzhi Qian
Jul 24, 2014·Molecules : a Journal of Synthetic Chemistry and Natural Product Chemistry·Jia-Yi FanHu-Biao Chen

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Citations

Mar 13, 2019·The American Journal of Chinese Medicine·Chao-Yong WangYuan-Zhong Wang
Oct 5, 2019·Current Pharmaceutical Design·Sonal Desai, Pratima Tatke
Apr 4, 2021·Molecules : a Journal of Synthetic Chemistry and Natural Product Chemistry·Caterina VicidominiGiovanni N Roviello
Jun 22, 2021·Spectrochimica Acta. Part A, Molecular and Biomolecular Spectroscopy·Yu-Gang DingYuan-Zhong Wang
Jul 2, 2021·Evidence-based Complementary and Alternative Medicine : ECAM·Jing HuXia Li
Aug 18, 2021·Journal of the Science of Food and Agriculture·Li WangYuanzhong Wang

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Methods Mentioned

BETA
electrophoresis

Software Mentioned

Similarity Evaluation System for Chromatographic Fingerprint

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