Free-film small-angle neutron scattering: a novel container-free in situ sample environment with minimized H/D exchange

Journal of Applied Crystallography
Sebastian W KraussMirijam Zobel

Abstract

The development of a container-free sample environment which is particularly well suited for in situ reaction studies of liquid samples by small-angle neutron scattering and related techniques is reported. Hydrogen exchange with the humidity from air is reduced by an encapsulating setup in a bag filled with an inert gas such as He. The effectiveness of this measure is quantitatively accessed by infrared absorption and gravimetry, and further correlated with neutron scattering.

References

Apr 1, 1988·Physical Review A: General Physics·K ToukanJ Teixeira
Feb 3, 2011·Langmuir : the ACS Journal of Surfaces and Colloids·Haiou QuCharles J O'Connor
Apr 19, 2011·The Journal of Chemical Physics·Johan QvistBertil Halle
Jan 17, 2015·Science·Mirijam ZobelSimon A J Kimber
Sep 4, 2015·Langmuir : the ACS Journal of Surfaces and Colloids·T SchindlerT Unruh
Jun 14, 2018·Journal of Applied Crystallography·Carlos G LopezJoão T Cabral

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Methods Mentioned

BETA
X-ray
SANS
neutron scattering
neutron inelastic scattering

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