Abstract
An improved method for the simultaneous determination of underivatized biogenic amines, cadaverine, putrescine, spermidine, histamine, tyramine and some amino acids precursors, histidine and tyrosine, in food products, based on ion-exchange chromatography (IC) with integrated pulsed amperometric detection (IPAD) has been developed. The method was successfully used for the analysis of biogenic amines and amino acids in food both of vegetable (kiwi, Actinidia chinensis) and animal origin, (fish, pilchard), as well as in fermented foods, such as cheese (Emmenthal) and dry sausages (salami). The method was also successfully used to study the changes in biogenic amines during the ripening of dry fermented sausages (salami). The analytes were extracted from foods with perchloric acid and the extracts were purified by liquid-liquid partition using n-hexane. Determination of biogenic amines was performed through cation-exchange chromatography with isocratic elution and IPAD. The detection limits for the analytes under investigation were found to range from 1.25 to 2.50 ng, at a signal-to-noise ratio of 3:1. Average recoveries ranged from 85.5 to 97.4% and R.S.D. values ranged from 3.4 to 8.8. The proposed method offers a number of adva...Continue Reading
References
Jun 1, 1979·Food and Cosmetics Toxicology·S L Taylor, E R Lieber
Apr 1, 1978·Food and Cosmetics Toxicology·L F BjeldanesM M Morris
May 25, 1990·Journal of Chromatography·S SuzukiK Takama
Nov 1, 1987·The Journal of Applied Bacteriology·R A EdwardsS V Ramantanis
Apr 4, 1986·Journal of Chromatography·H M Joosten, C Olieman
Sep 1, 1995·Letters in Applied Microbiology·I GeornarasA von Holy
Jun 17, 1955·Science·E GEIGER
Jul 27, 2006·Allergy·L GuglielmiP Demoly
Jan 1, 1995·Meat Science·R MaijalaA Fischer
Citations
Oct 12, 2012·Analytical and Bioanalytical Chemistry·Carmen PalermoDiego Centonze
May 17, 2005·Journal of Chromatography. B, Analytical Technologies in the Biomedical and Life Sciences·Hideyuki YoshidaMasatoshi Yamaguchi
Oct 31, 2002·Journal of Biochemical and Biophysical Methods·Livia NagyErno Lindner
Jul 18, 2000·International Journal of Food Microbiology·L Lehane, J Olley
Oct 4, 2002·Journal of Chromatography. B, Analytical Technologies in the Biomedical and Life Sciences·Jana LangeChristine Wittmann
May 9, 2012·Journal of Agricultural and Food Chemistry·Roberto Romero-GonzálezAntonia Garrido Frenich
Apr 8, 2004·Analytical Sciences : the International Journal of the Japan Society for Analytical Chemistry·Hideyuki YoshidaMasatoshi Yamaguchi
Jul 6, 2010·Journal of Chromatography. a·Giovanna Loredana La TorreGiacomo Dugo
Feb 26, 2010·Journal of Chromatography. a·Mark E ErupeKathleen L Purvis-Roberts
Aug 5, 2008·Journal of Chromatography. a·A KorösI Molnár-Perl
Mar 1, 2008·Journal of Chromatography. a·V GianottiM C Gennaro
Feb 18, 2006·Journal of Chromatography. a·J Ruiz-Jiménez, M D Luque de Castro
Jul 18, 2009·Analytical Sciences : the International Journal of the Japan Society for Analytical Chemistry·Ting-Fu JiangShuai Lian
Jun 15, 2011·Analytical Sciences : the International Journal of the Japan Society for Analytical Chemistry·Toshiyuki Suzuki, Michael A Quilliam
Feb 27, 2007·Journal of Chromatography. a·Brian M De Borba, Jeff S Rohrer
Jul 26, 2005·Journal of Chromatography. a·G SaccaniM Rey
Jul 29, 2011·Psychotherapy Research : Journal of the Society for Psychotherapy Research·Dana Atzil SlonimOrya Tishby
Aug 1, 2008·Zoonoses and Public Health·K SchwaigerJ Bauer
Apr 21, 2011·International Journal of Environmental Health Research·Karin SchwaigerJohann Bauer
Jan 7, 2010·Journal of Food Protection·Aniello AnastasioMaria Luisa Cortesi
Sep 9, 2000·The Medical Journal of Australia·L Lehane
Mar 7, 2021·Molecules : a Journal of Synthetic Chemistry and Natural Product Chemistry·Yun AiNing Zhang
Dec 5, 2000·Journal of Chromatography. B, Biomedical Sciences and Applications·A BouchereauF Larher
Nov 26, 2009·Journal of Agricultural and Food Chemistry·Eleonora MazzuccoMaria Carla Gennaro
Jun 20, 2021·Journal of Chromatography. a·Rajmund MichalskiJoanna Kernert