In situ analytical techniques for battery interface analysis

Chemical Society Reviews
Alok M TripathiBing Joe Hwang

Abstract

Lithium-ion batteries, simply known as lithium batteries, are distinct among high energy density charge-storage devices. The power delivery of batteries depends upon the electrochemical performances and the stability of the electrode, electrolytes and their interface. Interfacial phenomena of the electrode/electrolyte involve lithium dendrite formation, electrolyte degradation and gas evolution, and a semi-solid protective layer formation at the electrode-electrolyte interface, also known as the solid-electrolyte interface (SEI). The SEI protects electrodes from further exfoliation or corrosion and suppresses lithium dendrite formation, which are crucial needs for enhancing the cell performance. This review covers the compositional, structural and morphological aspects of SEI, both artificially and naturally formed, and metallic dendrites using in situ/in operando cells and various in situ analytical tools. Critical challenges and the historical legacy in the development of in situ/in operando electrochemical cells with some reports on state-of-the-art progress are particularly highlighted. The present compilation pinpoints the emerging research opportunities in advancing this field and concludes on the future directions and st...Continue Reading

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Citations

Nov 23, 2018·Physical Chemistry Chemical Physics : PCCP·Amund RuudHelmer Fjellvåg
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Oct 21, 2021·ACS Applied Materials & Interfaces·Kyungmi LimJoachim Maier

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Methods Mentioned

BETA
X-ray
electron spectroscopy
neutron scattering
neutron diffraction
coherent
neutron reflectometry
angle neutron scattering
SANS
inelastic neutron scattering
transmission

Software Mentioned

SECCM
ac
DEMS
SFG
SANS
SICM
SIMS
DRIFT
AFM
INS

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