KF-Silica as a stationary phase for the chromatographic removal of tin residues from organic compounds

Chemical Communications : Chem Comm
David C Harrowven, Ian L Guy

Abstract

Through the simple expedient of using a mixture of KF and silica as the stationary phase in column chromatography, levels of organotin impurities from tributyltin hydride mediated reductions have been reduced from stoichiometric levels to approximately 30 ppm.

References

Oct 4, 1996·The Journal of Organic Chemistry·David Crich, Sanxing Sun
Feb 16, 2002·The Journal of Organic Chemistry·Derrick L J Clive, Jian Wang
Dec 11, 2003·Organic & Biomolecular Chemistry·David C HarrowvenSteven Coulton
Sep 2, 2004·Chemical Communications : Chem Comm·David C HarrowvenMichael I T Nunn

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Citations

Sep 25, 2015·The Journal of Organic Chemistry·JongMyoung Chea, Derrick L J Clive
Sep 4, 2015·Chemical Reviews·Erwan Le GrognecJean-Paul Quintard
Sep 2, 2004·Chemical Communications : Chem Comm·David C HarrowvenMichael I T Nunn
Aug 29, 2012·Chemistry : a European Journal·Nikolay SitnikovHans-Günther Schmalz
May 3, 2008·Organic & Biomolecular Chemistry·Derrick L J Clive, Elia J L Stoffman
Oct 22, 2009·Chemistry : a European Journal·Haruaki KurasakiOsamu Tamura
Aug 18, 2010·Organic & Biomolecular Chemistry·Mark E WoodMichael B Hursthouse
Aug 25, 2010·Chemistry : a European Journal·Taku ShibueOsamu Tamura
Oct 21, 2010·Chemistry : a European Journal·Carolin Ammer, Thorsten Bach
Apr 6, 2019·Chemical Communications : Chem Comm·Jean-Baptiste VendevilleDavid C Harrowven
Jan 21, 2012·Chemistry : a European Journal·Max RoemerDieter Lentz
Nov 23, 2019·Molecules : a Journal of Synthetic Chemistry and Natural Product Chemistry·Nicolas MilliusPhilippe Renaud
Nov 13, 2008·Journal of the American Chemical Society·Barry M TrostArndt Meyer
Aug 9, 2008·The Journal of Organic Chemistry·Dan Fishlock, Robert M Williams
May 18, 2011·The Journal of Organic Chemistry·Gary D AingeGavin F Painter
Feb 6, 2007·The Journal of Organic Chemistry·Marie-Christine Matos, Paul V Murphy
Jun 17, 2005·Organic Letters·Anthony HayfordThomas Corprew

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