Measuring couplings in crowded NMR spectra: pure shift NMR with multiplet analysis

Chemical Communications : Chem Comm
Mohammadali ForoozandehG A Morris

Abstract

The PSYCHE method for pure shift NMR is exploited to generate 2D J spectra with full decoupling in one dimension and multiplet structure in the other, allowing spin-spin coupling constants to be measured even in very crowded spectra. Significant improvements over existing techniques are demonstrated for the hormones estradiol and androstenedione.

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