Multi-residue analysis of 90 emerging contaminants in liquid and solid environmental matrices by ultra-high-performance liquid chromatography tandem mass spectrometry

Journal of Chromatography. a
Bruce PetrieBarbara Kasprzyk-Hordern

Abstract

Reported herein is new analytical methodology for the determination of 90 emerging contaminants (ECs) in liquid environmental matrices (crude wastewater, final effluent and river water). The application of a novel buffer, ammonium fluoride improved signal response for several ECs determined in negative ionisation mode. Most notably the sensitivity of steroid estrogens was improved by 4-5 times in environmental extracts. Method recoveries ranged from 40 to 152% in all matrices and method quantitation limits (MQLs) achieved were <1ngL(-1) for numerous ECs. Development of a microwave assisted extraction (MAE) protocol as an additional sample extraction step for solid matrices enabled 63 ECs to be simultaneously analysed in digested sludge. To the authors knowledge this is considerably more than any previously reported MAE method. Here, MQLs ranged from 0.1-24.1ngg(-1) dry weight. The application of MAE offers several advantages over pressurized liquid extraction including faster sample preparation, lower solvent requirements, and the ability to perform several extractions simultaneously as well as lower purchasing and running costs. To demonstrate the method's sensitivity, application to environmental samples revealed 68 and 40 EC...Continue Reading

References

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Citations

Mar 15, 2016·Environmental Science & Technology·Bruce PetrieBarbara Kasprzyk-Hordern
Aug 21, 2016·Journal of Chromatography. B, Analytical Technologies in the Biomedical and Life Sciences·Ola Svahn, Erland Björklund
May 10, 2017·Environmental Toxicology and Chemistry·Emily E BurnsAlistair B A Boxall
Oct 5, 2018·Critical Reviews in Analytical Chemistry·M T García-CórcolesA Zafra-Gómez
Jan 10, 2019·Analytical and Bioanalytical Chemistry·Christina I NannouTriantafyllos A Albanis
Feb 24, 2019·Analytical and Bioanalytical Chemistry·Natalie SimsBarbara Kasprzyk-Hordern
Sep 21, 2016·Philosophical Transactions. Series A, Mathematical, Physical, and Engineering Sciences·Glenn LoosDeirdre Cabooter
Aug 18, 2017·Analytical and Bioanalytical Chemistry·Alexandros G AsimakopoulosKurunthachalam Kannan
Feb 24, 2020·Analytical and Bioanalytical Chemistry·Guilaine JariaValdemar I Esteves
Nov 8, 2017·Journal of Environmental Science and Health. Part A, Toxic/hazardous Substances & Environmental Engineering·Fernanda S SouzaLiliana A Féris
Apr 14, 2019·Molecules : a Journal of Synthetic Chemistry and Natural Product Chemistry·Ola Svahn, Erland Björklund
Mar 11, 2020·Environmental Science and Pollution Research International·Adebayo I Farounbi, Nosiphiwe P Ngqwala
Dec 1, 2019·Metabolites·Luca NarduzziGaud Dervilly-Pinel
Oct 13, 2018·The Science of the Total Environment·Bruce PetrieBarbara Kasprzyk-Hordern
Nov 19, 2018·The Science of the Total Environment·Samuel FekaduBart Van der Bruggen
Jan 29, 2019·Environment International·Luigi LopardoBarbara Kasprzyk-Hordern
Jan 16, 2021·Analytical Methods : Advancing Methods and Applications·Francesco RivaSara Castiglioni
Mar 16, 2018·Water Research·Emily E BurnsAlistair B A Boxall
Feb 26, 2021·Environmental Research·Martien H F GraumansPaul T J Scheepers
Mar 15, 2021·The Science of the Total Environment·G CastroI Rodríguez
Nov 6, 2020·Acta Pharmaceutica : a Quarterly Journal of Croatian Pharmaceutical Society and Slovenian Pharmaceutical Society, Dealing with All Branches of Pharmacy and Allied Sciences·Omar J Portillo-CastilloMarsela Garza-Tapia
Jun 8, 2021·Journal of Chromatography. B, Analytical Technologies in the Biomedical and Life Sciences·Benedikt RingbeckHolger M Koch

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