Multifaceted strategy for the synthesis of diverse 2,2'-bithiophene derivatives

Molecules : a Journal of Synthetic Chemistry and Natural Product Chemistry
Stanisław KrompiecAgnieszka Iwan

Abstract

New catalytically or high pressure activated reactions and routes, including coupling, double bond migration in allylic systems, and various types of cycloaddition and dihydroamination have been used for the synthesis of novel bithiophene derivatives. Thanks to the abovementioned reactions and routes combined with non-catalytic ones, new acetylene, butadiyne, isoxazole, 1,2,3-triazole, pyrrole, benzene, and fluoranthene derivatives with one, two or six bithiophenyl moieties have been obtained. Basic sources of crucial substrates which include bithiophene motif for catalytic reactions were 2,2'-bithiophene, gaseous acetylene and 1,3-butadiyne.

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Methods Mentioned

BETA
biosensor
X-ray
column chromatography
column

Software Mentioned

SCALE3
Olex2
SHELXS97
SHELXL97
ABSPACK

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