PMID: 9176938Feb 1, 1997Paper

Multiple-quantum magic-angle spinning NMR with cross-polarization: spectral editing of high-resolution spectra of quadrupolar nuclei

Solid State Nuclear Magnetic Resonance
M PruskiJ P Amoureux

Abstract

An experiment is presented that combines the multiple-quantum magic-angle spinning (MQMAS) technique with cross-polarization (CP). As a preliminary test of this new method, we measured and compared the 27Al 3QMAS and 19F-->27Al CP 3QMAS spectra of a fluorinated AlPO4 aluminophosphate. Complete discrimination between the fluorinated and nonfluorinated Al sites was easily achieved, which demonstrates the usefulness of CP MQMAS for spectral editing. Future applications of this experiment will include other spin pairs and heteronuclear correlation NMR spectroscopy.

References


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Citations

May 29, 1998·Solid State Nuclear Magnetic Resonance·J P Amoureux, C Fernandez
Aug 7, 1998·Solid State Nuclear Magnetic Resonance·S Steuernagel
Jan 23, 2013·Solid State Nuclear Magnetic Resonance·Frédéric A PerrasDavid L Bryce
Jan 11, 2011·Spectrochimica Acta. Part A, Molecular and Biomolecular Spectroscopy·Wen ZhangZhong Chen
Aug 24, 2010·Journal of Magnetic Resonance·C Vinod ChandranThomas Bräuniger
Jul 30, 2010·Progress in Nuclear Magnetic Resonance Spectroscopy·Redouane HajjarPascal P Man
Jan 10, 2009·Solid State Nuclear Magnetic Resonance·J P AmoureuxQ Wang
Jan 15, 2005·Journal of Magnetic Resonance·J P AmoureuxL Montagne
Dec 14, 2005·Solid State Nuclear Magnetic Resonance·Sean C ChristiansenBradley F Chmelka
Apr 13, 2002·Solid State Nuclear Magnetic Resonance·C FernandeM Pruski
Jun 23, 2015·Journal of the American Chemical Society·Frédéric A PerrasMarek Pruski
Dec 1, 2000·Journal of Magnetic Resonance·S E Ashbrook, S Wimperis
Nov 4, 1998·Journal of Magnetic Resonance·S Ding, C A McDowell
Sep 25, 1999·Journal of Magnetic Resonance·J C Chan
Feb 1, 2002·Journal of Magnetic Resonance·Adonis LupulescuHans Wolfgang Spiess
Jan 17, 2017·Solid State Nuclear Magnetic Resonance·Charlotte Martineau-CorcosFrancis Taulelle
Nov 17, 2017·The Journal of Chemical Physics·Diego CarnevaleGeoffrey Bodenhausen
Jan 13, 2012·Chemical Communications : Chem Comm·Veronika VitzthumGeoffrey Bodenhausen
Sep 29, 2011·Physical Chemistry Chemical Physics : PCCP·Aymeric SadocFlorent Boucher
Feb 21, 2009·Inorganic Chemistry·Charlotte MartineauEmmanuelle Suard

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