Note: development of fast heating inert gas annealing apparatus operated at atmospheric pressure

The Review of Scientific Instruments
S C DasRainer Hippler

Abstract

Here, we report the development of a simple, small, fast heating, and portable, homemade, inert gas (Ar) atmospheric annealing setup. Instead of using a conventional heating element, a commercial soldering rod having an encapsulated fast heating heater is used here. The sample holder is made of a block of stainless steel. It takes 200 s to reach 700 °C, and 10 min to cool down. The probability of oxidation or surface contamination has been examined by means of x ray photoelectron spectroscopy of virgin Cu sample after annealing at 600 °C. In addition, we compare the annealing of a hydrogenated carbon nitride film (HCN(x)) in both a conventional vacuum and our newly developed ambient Ar atmosphere setup.

References

Aug 4, 2007·The Review of Scientific Instruments·Abhijit Majumdar, Rainer Hippler
Oct 2, 2009·The Review of Scientific Instruments·Abhijit MajumdarRainer Hippler
Nov 10, 2009·The Journal of Physical Chemistry. B·Abhijit MajumdarRainer Hippler
Apr 5, 2011·The Review of Scientific Instruments·Georg EderMarkus Lackinger

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Citations

Nov 4, 2020·The Review of Scientific Instruments·Jitendra Kumar SinghRam Pyare

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Methods Mentioned

BETA
x ray photoelectron spectroscopy

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