Optimization of flocculation conditions for soluble cadmium removal using the composite flocculant of green anion polyacrylamide and PAC by response surface methodology

The Science of the Total Environment
Caifeng ZhaoLin Luo

Abstract

In this work, we describe a flocculation performance evaluation of a novel anionic polyacrylamide (APAM) synthesized using low dose γ-ray initiation. The APAM structure and morphology were characterized using Fourier transform-infrared spectroscopy (FTIR), High performance liquid chromatography (HPLC), thermogravimetric analysis (TGA), and scanning electron microscopy (SEM) techniques. In comparison to commercially purchased APAM (Mw = 1.0 × 107), γ-ray initiation was demonstrated to be a more effective method to increase molecular weight, decrease the residual acrylamide monomer, and improve thermal stability. Flocculant performance was evaluated by assessing their ability to remove Cd(II) from water. We utilized the Plackett-Burman (PB), steepest ascent, and response surface methodology (RSM) experimental design to identify the optimal flocculating conditions for the removal of soluble Cd(II). Under optimal conditions [26.84 mg L-1 CaO, 71.28 mg L-1 polyaluminium chloride (PAC) and 2.87 mg L-1 APAM], the maximum percent removal of Cd(II) was observed to reach 93.65%. A potential flocculation mechanism for the Cd(II) removal from water was further studied by evaluating the colloid Zeta potential. Results from these studies dem...Continue Reading

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