Storage effect of a pre-activated silane on the resin to ceramic bond

Dental Materials : Official Publication of the Academy of Dental Materials
Tabassom HooshmandAlireza Keshvad

Abstract

The purpose of this study was to investigate the process of hydrolysis and chemical stability of a pre-activated silane solution stored for different periods of time. The tensile bond strength of resin composite to ceramic was also evaluated in order to determine the functional effectiveness after storage of the pre-activated silane solutions. Silane solutions using gamma-methacryloxypropyltrimethoxysilane (gamma-MPTS), acetic acid and ethanol were freshly prepared and kept for 15 min, 2 h, 24 h, 1 week, 1 month, 6 months, and 1 year. The solutions were analyzed using a 2000 Perkin-Elmer Fourier transform infrared (FT-IR) spectrophotometer. For the tensile bond strength test, Ni/Cr rods were prepared with ceramic facings polished to 1 microm. Five groups of ceramic surfaces (n = 60) were treated with the pre-activated silane solutions and bonded using a luting resin. The process used to prepare the surfaces prior to bonding consisted of removing unreacted silane by boiling water and then heat treatment. Each group was then subdivided into two groups (n = 30) and stored under two different storage conditions before subjecting to the tensile bond strength test; either (1) dry at room temperature for 24 h or (2) boiling water for ...Continue Reading

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Citations

Jul 20, 2006·Journal of the Royal Society, Interface·Yuki ShirosakiAkiyoshi Osaka
May 25, 2012·Operative Dentistry·L H SilvaL F Valandro
Mar 13, 2014·Dental Materials : Official Publication of the Academy of Dental Materials·Tian TianMichael F Burrow
Jun 15, 2014·The Journal of Prosthetic Dentistry·Aljomar José Vechiato FilhoElidiane Cipriano Rangel
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Nov 6, 2012·Journal of the Mechanical Behavior of Biomedical Materials·Tabassom HooshmandFereshteh Zamani
Nov 1, 2011·Dental Materials : Official Publication of the Academy of Dental Materials·José Renato Cavalcanti QueirozMarco Antonio Bottino
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Nov 28, 2006·Dental Materials : Official Publication of the Academy of Dental Materials·Jukka P MatinlinnaPekka K Vallittu
Aug 23, 2008·Journal of Prosthodontics : Official Journal of the American College of Prosthodontists·Faride Gerami PanahLeila Ahmadian
Jun 22, 2007·Journal of Prosthodontics : Official Journal of the American College of Prosthodontists·Luciana A SalvioJonathan C Knowles
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Feb 12, 2005·Dental Materials : Official Publication of the Academy of Dental Materials·Jukka P MatinlinnaPekka K Vallittu
Mar 4, 2006·Journal of Dentistry·J P MatinlinnaP K Vallittu
Dec 21, 2005·Dental Materials : Official Publication of the Academy of Dental Materials·Francesca MonticelliMarco Ferrari
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Dec 1, 2017·Dental Materials : Official Publication of the Academy of Dental Materials·Raphael PiloGeorge Eliades
Mar 12, 2018·Dental Materials : Official Publication of the Academy of Dental Materials·Chenmin YaoCui Huang

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