Synthesis and application of a fluorous Lawesson's reagent: convenient chromatography-free product purification

Organic Letters
Zoltán KaletaTibor Soós

Abstract

[reaction: see text] A fluorous analogue of Lawesson's reagent for thionation of carbonyl compounds has been developed and its use demonstrated on a series of amides, esters, and ketones. The separation of the Lawesson's reagent-derived byproducts can be achieved by a simple fluorous solid-phase extraction.

References


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Citations

Jun 13, 2009·Chemical Communications : Chem Comm·Myung Gil ChoiSuk-Kyu Chang
Jul 9, 2016·Journal of Photochemistry and Photobiology. B, Biology·Rajesh SompalleMariadhas Valan Arasu
Apr 22, 2009·Molecular Diversity·C Oliver Kappe, Doris Dallinger
Jun 2, 2012·Dalton Transactions : an International Journal of Inorganic Chemistry·Jan Christopher Bernhammer, Han Vinh Huynh
Sep 18, 2007·Chemical Reviews·Turan OzturkOlcay Mert
Sep 20, 2007·Journal of Combinatorial Chemistry·Roland E DolleWei Zhang
Apr 24, 2021·Beilstein Journal of Organic Chemistry·Ke WuXinquan Hu
May 1, 2010·Chemical Reviews·Turan OzturkOlcay Mert
Feb 24, 2011·The Journal of Organic Chemistry·Jan BergmanPer H Svensson

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