Synthesis of Nitride Zeolites in a Hot Isostatic Press.

Angewandte Chemie
Sebastian WendlWolfgang Schnick

Abstract

The recently introduced nitridophosphate synthesis in a hot isostatic press (HIP) enabled simple access to large-scale product quantities starting from exclusively commercially available starting materials. Herein, we show that this method is suitable for the synthesis of highly condensed functional nitridophosphates, as well. Hence, the syntheses of the nitridophosphate zeolites Ba3 P5 N10 X (X=Cl, Br) are presented as proof of concept for this innovative access. Furthermore, samples of unprecedented Sr3 P5 N10 X (X=Cl, Br) were prepared and characterized to demonstrate the advantages of this synthetic approach over commonly used methods. Luminescence investigations on Eu2+ -doped samples of AE3 P5 N10 X (AE=Sr, Ba; X=Cl, Br) were carried out and characteristics of observed emission bands are discussed.

References

May 13, 2010·Chemistry : a European Journal·Florian J PucherWolfgang Schnick
Oct 19, 2010·Journal of the American Chemical Society·Jennifer A Armstrong, Mark T Weller
Jan 13, 2015·Angewandte Chemie·Alexey Marchuk, Wolfgang Schnick
Mar 15, 2015·Chemistry : a European Journal·Florian J PucherWolfgang Schnick
Sep 10, 2015·Angewandte Chemie·Simon David Kloss, Wolfgang Schnick
Dec 16, 2016·Chemistry : a European Journal·Eva-Maria BertschlerWolfgang Schnick
Oct 14, 2017·Chemistry : a European Journal·Eva-Maria BertschlerWolfgang Schnick
Jul 26, 2018·Chemistry : a European Journal·Mathias MallmannWolfgang Schnick
Aug 9, 2018·Angewandte Chemie·Sebastian VogelWolfgang Schnick
Nov 30, 2018·Angewandte Chemie·Simon D Kloß, Wolfgang Schnick
Jan 8, 2020·Chemistry : a European Journal·Mathias MallmannWolfgang Schnick
Feb 8, 2020·Chemistry : a European Journal·Sebastian WendlWolfgang Schnick
Apr 9, 2020·Chemistry : a European Journal·Sebastian WendlWolfgang Schnick
Jul 10, 2020·Angewandte Chemie·Sebastian WendlWolfgang Schnick

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