The determination of the extractability of selected elements from agricultural soil.

Environmental Monitoring and Assessment
Michaela ZeinerGerhard Stingeder

Abstract

Concentrations of Ag, Al, Ba, Cd, Co, Cr, Cu, Fe, K, Mn, Na, Ni, Pb, Sr, and Zn-isolated by sequential extraction steps from apple orchard soil-were analyzed by inductively coupled plasma-atomic emission spectroscopy and compared to the total amount of metal in soil determined by XRF. The extractable amount of each metal was calculated by the extraction yields of the four steps. The LODs of the different elements in all extracts ware below 3 μg/L except for Ba (steps 1 and 2), Cu (step 1), Fe (all steps), K (steps 1-3), Mn (step 2), Na (steps 1-3), Ni (step 1), Pb (steps 1 and 4), and Zn (steps 1 and 2). The highest LOD (>10 μg/L) was found for Fe, K, and Na (step 1). The recovery of all metals after four sequential extraction steps was 90-112%. The repeatability (<1.1%), the intermediate precision (<5.3%), the day-to-day reproducibility (<6.2%), and the overall uncertainty of measurement (approximately 4-8.5%) for all analyzed metals supports the choice of the method used.

References

Sep 26, 2002·Ecotoxicology and Environmental Safety·Rachel E PughArthur L Fredeen
Jun 17, 2006·Environmental Pollution·Neal W MenziesPeter M Kopittke
Apr 21, 2007·Ecotoxicology and Environmental Safety·Willie J G M PeijnenburgMartina G Vijver

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Citations

Dec 3, 2014·Journal of Pharmaceutical and Biomedical Analysis·Michaela ZeinerGerhard Stingeder
Apr 14, 2018·Environmental Monitoring and Assessment·Adam Łukowski, Dorota Dec
Jun 13, 2018·Toxics·Michaela Zeiner, Iva Juranović Cindrić

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