The HXD95: a modified Bassett-type hydrothermal diamond-anvil cell for in situ XRD experiments up to 5 GPa and 1300 K

Journal of Synchrotron Radiation
Marion LouvelSimone Anzellini

Abstract

A new diamond-anvil cell apparatus for in situ synchrotron X-ray diffraction measurements of liquids and glasses, at pressures from ambient to 5 GPa and temperatures from ambient to 1300 K, is reported. This portable setup enables in situ monitoring of the melting of complex compounds and the determination of the structure and properties of melts under moderately high pressure and high temperature conditions relevant to industrial processes and magmatic processes in the Earth's crust and shallow mantle. The device was constructed according to a modified Bassett-type hydrothermal diamond-anvil cell design with a large angular opening (θ = 95°). This paper reports the successful application of this device to record in situ synchrotron X-ray diffraction of liquid Ga and synthetic PbSiO3 glass to 1100 K and 3 GPa.

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Citations

Apr 28, 2020·Physical Review Letters·James W E DrewittOliver T Lord
Jul 11, 2021·The Review of Scientific Instruments·Benedict J HeinenOliver T Lord
Sep 21, 2021·Journal of Physics. Condensed Matter : an Institute of Physics Journal·James W E Drewitt

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Methods Mentioned

BETA
nuclear
X-ray
neutron diffraction
chips

Software Mentioned

DAWN

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