PMID: 11916398Mar 28, 2002Paper

Two-dimensional (13)C-(13)C correlation spectroscopy with magic angle spinning and dynamic nuclear polarization

Journal of the American Chemical Society
Melanie RosayRobert G Griffin

Abstract

The sensitivity of solid-state NMR experiments can be enhanced with dynamic nuclear polarization (DNP), a technique that transfers the high Boltzmann polarization of unpaired electrons to nuclei. Signal enhancements of up to 23 have been obtained for magic angle spinning (MAS) experiments at 5 T and 85-90 K using a custom-designed high-power gyrotron. The extended stability of MAS/DNP experiments at low temperature is demonstrated with (1)H-driven (13)C spin-diffusion experiments on the amino acid proline. These (13)C-(13)C chemical shift correlation spectra are the first two-dimensional MAS/DNP experiments performed at high field (>1.4 T).

References

Jul 17, 1998·Nature Structural Biology·R G Griffin
Dec 3, 1998·Journal of Biomolecular NMR·D L JakemanJ N Evans

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Citations

Feb 5, 2003·Journal of Magnetic Resonance·B Reif, R G Griffin
Mar 5, 2003·Journal of Magnetic Resonance·V S BajajR G Griffin
Apr 20, 2013·Accounts of Chemical Research·Qing Zhe NiRobert G Griffin
Mar 31, 2011·Journal of the American Chemical Society·Björn CorziliusRobert G Griffin
Aug 25, 2012·Journal of the American Chemical Society·Olesya HazeTimothy M Swager
Feb 21, 2013·The Journal of Physical Chemistry. B·Ta-Chung OngRobert G Griffin
Feb 9, 2007·The Journal of Chemical Physics·Kan-Nian HuRobert G Griffin
Aug 16, 2015·The Journal of Physical Chemistry Letters·Chandan SinghNeeraj Sinha
Jan 14, 2012·The Journal of Chemical Physics·Albert A SmithRobert G Griffin
Feb 13, 2008·The Journal of Chemical Physics·Thorsten MalyRobert G Griffin
Apr 5, 2011·The Journal of Chemical Physics·Kan-Nian HuRobert G Griffin
Feb 6, 2009·Applied Magnetic Resonance·A B BarnesR G Griffin
Aug 10, 2007·IEEE Transactions on Plasma Science·Melissa K HornsteinRichard J Temkin
Aug 29, 2011·IEEE Transactions on Terahertz Science and Technology·Emilio A NanniRichard J Temkin
Aug 19, 2015·Frontiers in Molecular Biosciences·Chen SongJörg Matysik
May 21, 2010·Physical Chemistry Chemical Physics : PCCP·R G Griffin, T F Prisner
Aug 9, 2013·Physical Chemistry Chemical Physics : PCCP·Shamon A WalkerSongi Han
Mar 30, 2013·Journal of Infrared, Millimeter and Terahertz Waves·Sudheer JawlaRichard Temkin
May 8, 2010·Physical Chemistry Chemical Physics : PCCP·Melanie RosayWerner E Maas
Oct 22, 2018·The Journal of Chemical Physics·Frédéric A Perras, Marek Pruski
Jun 27, 2014·Physical Chemistry Chemical Physics : PCCP·Ting Ann SiawSong-I Han
Jun 13, 2019·Solid State Nuclear Magnetic Resonance·Andrew G M RankinOlivier Lafon
Nov 22, 2005·Solid State Nuclear Magnetic Resonance·V Weis, R G Griffin
Nov 8, 2013·The Journal of Physical Chemistry. B·Vladimir K MichaelisRobert G Griffin
Jun 2, 2015·Journal of the American Chemical Society·Rahul P SangodkarBradley F Chmelka
Aug 2, 2017·The Journal of Physical Chemistry. B·Qing Zhe NiYongchao Su
Oct 2, 2012·The Journal of Physical Chemistry Letters·Vladimir K MichaelisRobert G Griffin
Aug 31, 2006·Journal of the American Chemical Society·Changsik SongRobert G Griffin
Sep 2, 2004·Journal of the American Chemical Society·Kan-Nian HuRobert G Griffin
Nov 6, 2003·Journal of the American Chemical Society·Melanie RosayRobert G Griffin
Aug 17, 2006·Journal of the American Chemical Society·Patrick C A van der WelRobert G Griffin

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